2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester

Base Information

• Chemical Name: 2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester
• CAS No.: 106805-50-9
• Molecular Formula: C₂₁H₆Cl₄I₄O₅
• Molecular Weight: 987.706

Synonyms:2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester

Chemical Property of 2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester

Chemical Property:

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Technology Process of 2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester

There total 1 articles about 2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.8%

rose bengal (632-69-9) + methyl iodide (74-88-4) → 2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester (106805-50-9)

Guidance literature:

With hydrogenchloride; tetrabutyl-ammonium chloride; In tetrahydrofuran; for 12h; Heating;

DOI:10.1016/S0040-4020(01)86891-5

Reference yield:

2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester (106805-50-9) → 2,3,4,5-Tetrachloro-6-(3,6-dihydroxy-2,7-diiodo-9H-xanthen-9-yl)-benzoic acid methyl ester

Guidance literature:

With acetic acid; zinc; at 60 ℃; for 2h;

DOI:10.1016/S0040-4020(01)86891-5

Reference yield:

2,3,4,5-Tetrachloro-6-(6-hydroxy-2,4,5,7-tetraiodo-3-oxo-3H-xanthen-9-yl)-benzoic acid methyl ester (106805-50-9) → 2,3,4,5-Tetrachloro-6-(3,6-dihydroxy-2,4,5,7-tetraiodo-9H-xanthen-9-yl)-benzoic acid methyl ester

Guidance literature:

With triethanolamine; In 1,2-dimethoxyethane; for 4h; Irradiation;

DOI:10.1016/S0040-4020(01)86891-5

upstream raw materials:

rose bengal

methyl iodide

Downstream raw materials:

2-(3-Acetoxy-6-hydroxy-9H-xanthen-9-yl)-3,4,5,6-tetrachloro-benzoic acid methyl ester

2-(3-Acetoxy-6-hydroxy-2,7-diiodo-9H-xanthen-9-yl)-3,4,5,6-tetrachloro-benzoic acid methyl ester

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