N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide

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Chemical Name:N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide
CAS No.:123845-17-0
Molecular Formula:C₃₀H₃₄N₄O₆S₄
Molecular Weight:674.887
Hs Code.:

Synonyms:N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide

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Chemical Property of N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide

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Technology Process of N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide

There total 3 articles about N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 134469-06-0
thiazolidine-2-thione

: 123845-15-8
[(Benzyl-{2-[benzyl-(2-carboxymethoxy-acetyl)-amino]-ethyl}-carbamoyl)-methoxy]-acetic acid

: 123845-17-0
N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In ethyl acetate; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80444-0

Reference yield: 39.0%

: 123845-15-8
[(Benzyl-{2-[benzyl-(2-carboxymethoxy-acetyl)-amino]-ethyl}-carbamoyl)-methoxy]-acetic acid

: 96-53-7
2-mercaptothiazoline

: 123845-17-0
N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1016/S0040-4039(00)99467-X

Reference yield:

: 140-28-3,87170-83-0
N,N'-Dibenzylethylenediamine

: 123845-17-0
N-Benzyl-N-[2-(benzyl-{2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetyl}-amino)-ethyl]-2-[2-oxo-2-(2-thioxo-thiazolidin-3-yl)-ethoxy]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / tetrahydrofuran / 12 h / 50 °C

2: 71 percent / dicyclohexylcarbodiimide, 4-dimethylaminopyridine / ethyl acetate / 24 h / Ambient temperature

With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/S0040-4020(01)80444-0