C₂₁H₃₀N₂O₆

Base Information

• Chemical Name: C₂₁H₃₀N₂O₆
• CAS No.: 939435-76-4
• Molecular Formula: C₂₁H₃₀N₂O₆
• Molecular Weight: 406.479
• Mol file: 939435-76-4.mol

Synonyms:C₂₁H₃₀N₂O₆

Chemical Property of C₂₁H₃₀N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₃₀N₂O₆

There total 1 articles about C₂₁H₃₀N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C14H23NO6 (145773-74-6) + N-benzyloxyamine (622-33-3) → C21H30N2O6 (939435-76-4)

Guidance literature:

C₁₄H₂₃NO₆; With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 4 - 20 ℃;

N-benzyloxyamine; In N,N-dimethyl-formamide; for 14h; Further stages.;

DOI:10.1021/jm061082q

Reference yield: 94.0%

C21H30N2O6 (939435-76-4) → C20H30N2O6 (939435-77-5)

Guidance literature:

With lithium hydroxide; In methanol; at 0 ℃; for 1h;

DOI:10.1021/jm061082q

Reference yield:

C21H30N2O6 (939435-76-4) → C33H54N4O10Si

Guidance literature:

Multi-step reaction with 3 steps

1: 94 percent / aq. LiOH / methanol / 1 h / 0 °C

2: 68 percent / DIEA; [(7-azabenzotriazol-1-yloxy) 1-tripyrrolidino]P*PF₆ / dimethylformamide / 16 h / 20 °C

3: H₂ / Pd/BaSO₄ / methanol / 3 h / 20 °C / 517.16 Torr

With lithium hydroxide; hydrogen; N-ethyl-N,N-diisopropylamine; Pd-BaSO₄; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/jm061082q

upstream raw materials:

C₁₄H₂₃NO₆

N-benzyloxyamine

Downstream raw materials:

C₂₀H₃₀N₂O₆

C₄₀H₆₀N₄O₁₀Si

C₃₀H₃₈N₄O₇

C₃₀H₄₁N₃O₇