(3S,4R,5S,6S)-6-(3-(4-acetoxybenzyl)-4-chlorophenyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl tetraacetate

Base Information

Chemical Name:(3S,4R,5S,6S)-6-(3-(4-acetoxybenzyl)-4-chlorophenyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl tetraacetate
CAS No.:1309963-55-0
Molecular Formula:C₂₈H₂₉ClO₁₁
Molecular Weight:576.985
Hs Code.:

Synonyms:(3S,4R,5S,6S)-6-(3-(4-acetoxybenzyl)-4-chlorophenyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl tetraacetate

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Chemical Property of (3S,4R,5S,6S)-6-(3-(4-acetoxybenzyl)-4-chlorophenyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl tetraacetate

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Technology Process of (3S,4R,5S,6S)-6-(3-(4-acetoxybenzyl)-4-chlorophenyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl tetraacetate

There total 6 articles about (3S,4R,5S,6S)-6-(3-(4-acetoxybenzyl)-4-chlorophenyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: ((3aS,5S,6R,6aS)-6-((tert-butyldimethylsilyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)(3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-chlorophenyl)methanol

: 108-24-7
acetic anhydride

: 64-19-7,77671-22-8
acetic acid

: 1309963-55-0
(3S,4R,5S,6S)-6-(3-(4-acetoxybenzyl)-4-chlorophenyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl tetraacetate

Guidance literature:: ((3aS,5S,6R,6aS)-6-((tert-butyldimethylsilyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)(3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-chlorophenyl)methanol; acetic acid; In water; acetic acid; at 110 ℃; for 22h;

acetic anhydride; With pyridine; In toluene; at 20 ℃; for 16h;

Reference yield: 70.0%

: ((3aS,6R,6aS)-6-((tert-butyldimethylsilyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)(3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-chlorophenyl)methanol

: 108-24-7
acetic anhydride

: 1309963-55-0
(3S,4R,5S,6S)-6-(3-(4-acetoxybenzyl)-4-chlorophenyl)tetrahydro-2H-pyran-2,3,4,5-tetrayl tetraacetate

Guidance literature:: ((3aS,6R,6aS)-6-((tert-butyldimethylsilyl)oxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)(3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-chlorophenyl)methanol; With water; acetic acid; at 110 ℃; for 22h;

acetic anhydride; With pyridine; at 20 ℃; for 16h;