1-(2-chlorobenzyl)indole-3-carboxaldehyde thiocarbohydrazone

Base Information

Chemical Name:1-(2-chlorobenzyl)indole-3-carboxaldehyde thiocarbohydrazone
CAS No.:1598435-78-9
Molecular Formula:C₁₇H₁₆ClN₅S
Molecular Weight:357.867
Hs Code.:

Synonyms:1-(2-chlorobenzyl)indole-3-carboxaldehyde thiocarbohydrazone

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Chemical Property of 1-(2-chlorobenzyl)indole-3-carboxaldehyde thiocarbohydrazone

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Technology Process of 1-(2-chlorobenzyl)indole-3-carboxaldehyde thiocarbohydrazone

There total 2 articles about 1-(2-chlorobenzyl)indole-3-carboxaldehyde thiocarbohydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2231-57-4
Thiocarbohydrazide

: 90815-00-2
1-(2-chlorobenzyl)-1H-indole-3-carbaldehyde

: 1598435-78-9
1-(2-chlorobenzyl)indole-3-carboxaldehyde thiocarbohydrazone

Guidance literature:: Thiocarbohydrazide; With acetic acid; In water; at 90 ℃;

1-(2-chlorobenzyl)-1H-indole-3-carbaldehyde; In ethanol; water; for 1h; Reflux;
DOI:10.1111/cbdd.12230

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 1598435-78-9
1-(2-chlorobenzyl)indole-3-carboxaldehyde thiocarbohydrazone

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / dimethyl sulfoxide / 0.08 h

2.1: acetic acid / water / 90 °C

2.2: 1 h / Reflux

With potassium carbonate; acetic acid; In water; dimethyl sulfoxide;
DOI:10.1111/cbdd.12230