4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate

Base Information

Chemical Name:4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate
CAS No.:123715-72-0
Molecular Formula:C₃₁H₄₀O₆
Molecular Weight:508.655
Hs Code.:

Synonyms:4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate

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Chemical Property of 4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate

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Technology Process of 4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate

There total 1 articles about 4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 123715-64-0
4β,5-cyclopropano-5β-androstane-3β,17β,19-triol 3-acetate 17-benzoate 19-p-toluenesulfonate

: 123715-67-3
4β,5-cyclopropano-5(10a)-homo-19-nor-5β-adrosta-1(10),2-dien-17β-ol 17-benzoate

: 123715-70-8
4β,5-cyclopropano-5(10a)-homo-19-nor-5β-adrosta-1(10)-ene-3α,17β-diol 3-acetate 17-benzoate

: 123715-72-0
4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate

Guidance literature:: With potassium acetate; In acetic anhydride; acetic acid; 1.)reflux, 4 h 2.)add H₂O, reflux, 30 min;

Reference yield: 46.0%

: 123715-72-0
4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate

: 123715-71-9
4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 5-acetate 17-benzoate

Guidance literature:: With potassium carbonate; In methanol; water; at 35 ℃; for 4h;

Reference yield:

: 123715-72-0
4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstane-3β,5,17β-triol 3,5-diacetate 17-benzoate

: 123715-77-5
5,17β-dihydroxy-4β,10β-cyclo-5(10a)-homo-19-nor-5β-androstan-3-one 5-acetate 17-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / K₂CO₃ / methanol; H₂O / 4 h / 35 °C

2: 83 percent / Jones' reagent / acetone / 0.17 h / Ambient temperature

With jones' reagent; potassium carbonate; In methanol; water; acetone;