C₂₉H₂₆FNO₆S

Base Information

Chemical Name:C₂₉H₂₆FNO₆S
CAS No.:1374234-45-3
Molecular Formula:C₂₉H₂₆FNO₆S
Molecular Weight:535.593
Hs Code.:

C<sub>29</sub>H<sub>26</sub>FNO<sub>6</sub>S

Synonyms:C₂₉H₂₆FNO₆S

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Chemical Property of C₂₉H₂₆FNO₆S

Chemical Property:

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Technology Process of C₂₉H₂₆FNO₆S

There total 11 articles about C₂₉H₂₆FNO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1374234-44-2
C₃₀H₂₇F₄NO₉S₂

: 1374234-45-3
C₂₉H₂₆FNO₆S

Guidance literature:: With triethylamine; lithium chloride; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 120 ℃; for 2h; Inert atmosphere;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374234-45-3
C₂₉H₂₆FNO₆S

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

7.1: pyridine / dichloromethane / 3 h / 0 °C

8.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

9.1: boron trichloride / dichloromethane / 2 h / -30 °C / Inert atmosphere

9.2: Cooling with ice

10.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 0 - 20 °C

11.1: triethylamine; lithium chloride / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 2 h / 120 °C / Inert atmosphere

With pyridine; potassium phosphate; hydrogen; nitric acid; boron trichloride; sodium hydride; potassium carbonate; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; zinc(II) chloride; dmap; palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374234-45-3
C₂₉H₂₆FNO₆S

Guidance literature:: Multi-step reaction with 10 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 3 h / 20 °C

6.1: pyridine / dichloromethane / 3 h / 0 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

8.1: boron trichloride / dichloromethane / 2 h / -30 °C / Inert atmosphere

8.2: Cooling with ice

9.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 0 - 20 °C

10.1: triethylamine; lithium chloride / palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 2 h / 120 °C / Inert atmosphere

With pyridine; potassium phosphate; hydrogen; nitric acid; boron trichloride; potassium carbonate; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; lithium chloride; zinc(II) chloride; dmap; palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; tert-butyl XPhos; In 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;