4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene

Base Information

Chemical Name:4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene
CAS No.:548735-31-5
Molecular Formula:C₂₀H₃₃BrO₃
Molecular Weight:401.384
Hs Code.:

Synonyms:4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene

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Chemical Property of 4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene

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Technology Process of 4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene

There total 3 articles about 4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.6%

: 6296-63-5
4-bromo-2,6-bis(hydroxymethyl)phenol

: 143-15-7
1-dodecylbromide

: 548735-31-5
4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene

Guidance literature:: With potassium carbonate; In acetone; for 48h; Heating;
DOI:10.1021/ja021233o

Reference yield:

: 106-41-2
4-bromo-phenol

: 548735-31-5
4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 63.4 percent / aq. KOH / propan-2-ol / 89 h / 40 °C

2: 74.6 percent / K₂CO₃ / acetone / 48 h / Heating

With potassium hydroxide; potassium carbonate; In isopropyl alcohol; acetone;
DOI:10.1021/ja021233o

Reference yield:

: 106-41-2
4-bromo-phenol

: 548735-31-5
4-bromo-2,6-bis(hydroxymethyl)-1-dodecyloxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / water; isopropyl alcohol / 89 h / 40 °C

2: potassium carbonate / acetone / 48 h / Reflux

With potassium carbonate; potassium hydroxide; In water; isopropyl alcohol; acetone;
DOI:10.1016/j.polymer.2014.11.042