8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Base Information

Chemical Name:8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside
CAS No.:1061303-17-0
Molecular Formula:C₂₉H₄₀O₁₃
Molecular Weight:596.629
Hs Code.:

Synonyms:8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

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Technology Process of 8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

There total 1 articles about 8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1061303-14-7
8-(4-allyloxyphenyl)-3,6-dioxaoctanol

: 4163-60-4
β-D-galactose peracetate

: 1061303-17-0
8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In propiononitrile; at 0 - 20 ℃; for 12h;
DOI:10.1016/j.bmc.2008.08.076

Reference yield: 82.0%

: 1061303-17-0
8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

: 100-39-0
benzyl bromide

: 1061303-19-2
8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranoside

Guidance literature:: 8-(4-allyloxyphenyl)-3,6-dioxaoctyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside; With sodium methylate; In methanol; for 2h;

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

benzyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.bmc.2008.08.076