1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid

Base Information

Chemical Name:1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid
CAS No.:1567898-20-7
Molecular Formula:C₁₉H₂₈N₂O₅S
Molecular Weight:396.508
Hs Code.:

Synonyms:1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid

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Chemical Property of 1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid

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Technology Process of 1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid

There total 4 articles about 1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3253-43-8
Spiro<4.5>decan-2,4'-oxazolidine-2,5'-dione

: 649-15-0
N,N-diethyl-4-methylbenzenesulfonamide

: 1567898-20-7
1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid

Guidance literature:: N,N-diethyl-4-methylbenzenesulfonamide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

Spiro<4.5>decan-2,4'-oxazolidine-2,5'-dione; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol500523n

Reference yield:

: 2756-85-6
1-aminocyclohexane carboxylic acid

: 1567898-20-7
1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 3 h / 50 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1021/ol500523n

Reference yield:

: 115951-16-1
1-tert-butoxycarbonylaminocyclohexanecarboxylic acid

: 1567898-20-7
1-(2-(N,N-diethylsulfamoyl)-5-methylbenzamido)cyclohexanecarboxylicacid

Guidance literature:: Multi-step reaction with 2 steps

1.1: phosphorus trichloride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

With n-butyllithium; phosphorus trichloride; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol500523n