1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole

Base Information

Chemical Name:1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole
CAS No.:1333492-74-2
Molecular Formula:C₃₉H₂₈N₆
Molecular Weight:580.692
Hs Code.:

Synonyms:1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole

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Chemical Property of 1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole

There total 5 articles about 1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 446852-65-9
2-(2-bromopyridin-4-yl)-1-(pyridin-2-yl)ethan-1-one

: 1333492-74-2
1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / N,N-dimethyl-formamide / 0.08 h / Inert atmosphere

1.2: 1.5 h / Inert atmosphere

2.1: hydrazine hydrate / N,N-dimethyl-formamide / 24 h / 20 - 50 °C / Inert atmosphere

3.1: triethylamine / dichloromethane

4.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / 230 °C / Microwave irradiation

With potassium carbonate; hydrazine hydrate; acetic acid; triethylamine; In 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.120

Reference yield:

: (E)-2-(2-Bromo-pyridin-4-yl)-3-dimethylamino-1-pyridin-2-yl-propenone

: 1333492-74-2
1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / N,N-dimethyl-formamide / 24 h / 20 - 50 °C / Inert atmosphere

2: triethylamine / dichloromethane

3: potassium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / 230 °C / Microwave irradiation

With potassium carbonate; hydrazine hydrate; triethylamine; In 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.120

Reference yield:

: 4926-28-7
2-Bromo-4-picoline

: 1333492-74-2
1-(4-(3-(pyridin-2-yl)-1-trityl-1H-pyrazol-4-yl)pyridin-2-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -50 °C / Inert atmosphere

1.2: -50 - 45 °C / Inert atmosphere

2.1: acetic acid / N,N-dimethyl-formamide / 0.08 h / Inert atmosphere

2.2: 1.5 h / Inert atmosphere

3.1: hydrazine hydrate / N,N-dimethyl-formamide / 24 h / 20 - 50 °C / Inert atmosphere

4.1: triethylamine / dichloromethane

5.1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / 230 °C / Microwave irradiation

With potassium hexamethylsilazane; potassium carbonate; hydrazine hydrate; acetic acid; triethylamine; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2010.12.120