3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one

Base Information

Chemical Name:3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one
CAS No.:1615687-56-3
Molecular Formula:C₂₆H₂₃N₃O₂
Molecular Weight:409.488
Hs Code.:

Synonyms:3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one

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Chemical Property of 3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one

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Technology Process of 3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one

There total 7 articles about 3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4894-26-2
3,4-dihydro-β-carboline

: 6-(benzyloxy)-1-methyl-1H-benzo[d][1,3]oxazine-2,4-dione

: 1615687-56-3
3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one

Guidance literature:: In dichloromethane; for 20h; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2014.05.002

Reference yield:

: 394-31-0
2-amino-5-hydroxybenzoic acid

: 1615687-56-3
3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,4-dioxane / 3 h / 108 °C / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

3.1: potassium hydroxide / water / 2 h / 95 °C / Inert atmosphere

4.1: Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 0.17 h / Inert atmosphere

5.2: 45 °C / Inert atmosphere

6.1: dichloromethane / 20 h / Inert atmosphere; Reflux

With potassium carbonate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In 1,4-dioxane; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.05.002

Reference yield:

: 104356-42-5
5-(benzyloxy)-2-((ethoxycarbonyl)amino)benzoic acid

: 1615687-56-3
3-(benzyloxy)-14-methyl-7,8,13b,14-tetrahydroindolo[20,30:3,4]pyrido[2,1-b]quinazolin-5(13H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 0.17 h / Inert atmosphere

2.2: 45 °C / Inert atmosphere

3.1: dichloromethane / 20 h / Inert atmosphere; Reflux

With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl acetamide;
DOI:10.1016/j.ejmech.2014.05.002