(E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate

Base Information

Chemical Name:(E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate
CAS No.:1108603-62-8
Molecular Formula:C₁₅H₁₈O₃
Molecular Weight:246.306
Hs Code.:

Synonyms:(E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate

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Chemical Property of (E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate

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Technology Process of (E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate

There total 1 articles about (E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-54-1
3-Phenylpropenol

: 26638-94-8
C₆H₈O₂

: 1108603-62-8
(E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate

Guidance literature:: With dmap;
DOI:10.1002/ejoc.200800854

Reference yield: 70.0%

: 1108603-62-8
(E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate

: 2-methyl-5-phenylhept-6-en-3-one

: C₂₄H₂₆O₃

Guidance literature:: With [Ru^IIcyclopentadienyl((R,R)-(3aS,11a-S,14aR,16bR)-2,2,13,13-tetraisopropyl-3a,11a,14a,16b-tetrahydrobis(1,3-dioxolano[4’,5’:3,4]pyrrolo)[1,2-a:1’,2’-a]naphtho[1,2-d:8,7-d’]diimidazole)]hexafluorophosphate; In dichloromethane; acetone; at 60 ℃; for 18h; enantioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.tet.2019.130888

Reference yield:

: 1108603-62-8
(E)-3-phenylprop-2-en-1-yl 4-methyl-3-oxopentanoate

: (+)-2-methyl-5-phenylhept-6-en-3-one

: (-)-2-methyl-5-phenylhept-6-en-3-one

: 872672-40-7
C₁₄H₁₈O

Guidance literature:: With (η⁵-cyclopentadienyl) (η⁶-naphthalene)ruthenium hexafluorophosphate; 2-(3aR,8aS)-(pyridin-2-yl)-8,8a-dihydro-3aH-indeno[1,2-d]oxazole; In tetrahydrofuran; at 60 ℃; for 9h; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/ejoc.200800854