(S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(benzyloxy)phenyl]ethylamine

Base Information

• Chemical Name: (S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(benzyloxy)phenyl]ethylamine
• CAS No.: 1258852-42-4
• Molecular Formula: C₃₅H₄₃NO₄Si
• Molecular Weight: 569.816

Synonyms:(S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(benzyloxy)phenyl]ethylamine

Chemical Property of (S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(benzyloxy)phenyl]ethylamine

Chemical Property:

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Technology Process of (S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(benzyloxy)phenyl]ethylamine

There total 1 articles about (S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(benzyloxy)phenyl]ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(S)-2-amino-1-[3,4,5-tris(benzyloxy)phenyl]ethanol (1258852-40-2) + tert-butyldimethylsilyl chloride (18162-48-6) → (S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(benzyloxy)phenyl]ethylamine (1258852-42-4)

Guidance literature:

With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ja105221u

Reference yield:

(S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(benzyloxy)phenyl]ethylamine (1258852-42-4) → (S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(hydroxy)phenyl]ethylamine (1258852-44-6)

Guidance literature:

With 5% Pd(II)/C(eggshell); hydrogen; In ethanol; at 20 ℃; for 24h; under 760.051 Torr;

DOI:10.1021/ja105221u

upstream raw materials:

(S)-2-amino-1-[3,4,5-tris(benzyloxy)phenyl]ethanol

tert-butyldimethylsilyl chloride

Downstream raw materials:

(S)-2-(tert-butyldimethylsiloxy)-2-[3,4,5-tris(hydroxy)phenyl]ethylamine

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