Technology Process of C20H24O2
There total 5 articles about C20H24O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 1h;
DOI:10.1039/c39940001151
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butoxide; n-BuLi / tetrahydrofuran; hexane / 0.17 h / -45 °C
1.2: (-)-methoxydiisopinocampheylborane / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.3: 56 percent / boron trifluoride etherate / tetrahydrofuran; hexane / 3 h / -78 °C
2.1: tetrabutylammonium iodide; NaH / dimethylformamide; various solvent(s) / 0.5 h / 0 °C
2.2: 1.34 g / dimethylformamide; various solvent(s) / 0 - 20 °C
With
n-butyllithium; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide;
1.1: Brown crotylboration / 1.2: Brown crotylboration / 1.3: Brown crotylboration;
DOI:10.1021/ja004154q
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) O3, 2.) Me2S / 1.) CH2Cl2, -78 deg C, 1.5 h, 2.) CH2Cl2, from - 78 deg C to RT, 22 h
2: 1.) tBuOK, n-BuLi, 2.) (-)-β-methoxydiisopinocampheylborane, 3.) BF3*Et2O, 4.) 3N aq. NaOH, 30percent aq. H2O2
3: 1.) KH / 1.) DMF, from 0 deg C to RT, 2.) DMF, 0 deg C, 1.5 h
With
sodium hydroxide; n-butyllithium; dimethylsulfide; boron trifluoride diethyl etherate; potassium tert-butylate; dihydrogen peroxide; potassium hydride; ozone; (-)-B-methoxydiisopinocampheylborane;
