5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine

Base Information

Chemical Name:5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine
CAS No.:175013-60-2
Molecular Formula:C₃₃H₃₄BrN₃O₇Si
Molecular Weight:692.638
Hs Code.:

Synonyms:5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine

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Chemical Property of 5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine

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Technology Process of 5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine

There total 5 articles about 5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 957-75-5
5-bromouridine

: 175013-60-2
5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / diphenylcarbonate, NaHCO₃ / dimethylformamide / 2 h / 80 °C

2: 40 percent / pyridine / Ambient temperature

3: pyridine

4: pyridine / 72 h

With pyridine; bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(96)00870-8

Reference yield:

: 35837-20-8
2',3'-anhydro-1-β-D-arabinofuranosyl-5-bromo-uracil

: 175013-60-2
5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / pyridine / Ambient temperature

2: pyridine

3: pyridine / 72 h

With pyridine;
DOI:10.1016/0040-4020(96)00870-8

Reference yield:

: 175013-57-7
(2R,3R,3aS,9aR)-7-Bromo-2-(tert-butyl-diphenyl-silanyloxymethyl)-3-hydroxy-2,3,3a,9a-tetrahydro-furo[2',3':4,5]oxazolo[3,2-a]pyrimidin-6-one

: 175013-60-2
5-bromo-3'-O-benzyloxyaminocarbonyl-5'-O-tert-butydiphenylsilyl-2,2'-O-anhydrouridine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: pyridine / 72 h

With pyridine;
DOI:10.1016/0040-4020(96)00870-8