C₂₂H₃₀O

Base Information

Chemical Name:C₂₂H₃₀O
CAS No.:1631040-47-5
Molecular Formula:C₂₂H₃₀O
Molecular Weight:310.48
Hs Code.:

Synonyms:C₂₂H₃₀O

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Chemical Property of C₂₂H₃₀O

Chemical Property:

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Technology Process of C₂₂H₃₀O

There total 6 articles about C₂₂H₃₀O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1631040-46-4
C₂₂H₃₀O

: 1631040-47-5
C₂₂H₃₀O

Guidance literature:: With Echavarren's catalyst; In dichloromethane; at 23 ℃; for 0.0833333h; Temperature; Time; Inert atmosphere;
DOI:10.1002/anie.201402044

Reference yield: 56.0%

: 1631040-46-4
C₂₂H₃₀O

: 107-18-6
allyl alcohol

: 1631040-48-6
C₁₈H₂₈O

: 1631040-47-5
C₂₂H₃₀O

Guidance literature:: With Echavarren's catalyst; In dichloromethane; for 0.25h; Inert atmosphere;
DOI:10.1002/anie.201402044

Reference yield:

: 106-28-5
Farnesol

: 1631040-47-5
C₂₂H₃₀O

Guidance literature:: Multi-step reaction with 5 steps

1.1: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate / dichloromethane; tert-butyl alcohol / -48 °C / Molecular sieve; Inert atmosphere

2.1: triphenylphosphine; sodium hydrogencarbonate; tetrachloromethane / 6 h / Inert atmosphere; Reflux

3.1: n-butyllithium / tetrahydrofuran / 2 h / -40 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

5.1: Echavarren's catalyst / dichloromethane / 0.08 h / 23 °C / Inert atmosphere

With titanium(IV) isopropylate; tetrachloromethane; n-butyllithium; Echavarren's catalyst; L-(+)-diisopropyl tartrate; sodium hydride; sodium hydrogencarbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; mineral oil; tert-butyl alcohol;
DOI:10.1002/anie.201402044