4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester

Base Information

• Chemical Name: 4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester
• CAS No.: 59100-11-7
• Molecular Formula: C₂₇H₄₆O₆S
• Molecular Weight: 498.725
• Mol file: 59100-11-7.mol

Synonyms:4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester

Chemical Property of 4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester

There total 3 articles about 4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

18-bromooctadecan-1-ol (59101-17-6) → 4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester (59100-11-7)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOMe / methanol / Heating

2: Py

With pyridine; sodium methylate; In methanol;

DOI:10.1021/jm00229a018

Reference yield:

18-bromooctadecanoic acid (2536-38-1) → 4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester (59100-11-7)

Guidance literature:

Multi-step reaction with 3 steps

1: B₂H₆ / tetrahydrofuran / Ambient temperature

2: NaOMe / methanol / Heating

3: Py

With pyridine; sodium methylate; diborane; In tetrahydrofuran; methanol;

DOI:10.1021/jm00229a018

Reference yield:

4-(18-Hydroxy-octadecyloxy)-benzoic acid methyl ester (59100-04-8) + methanesulfonyl chloride (124-63-0) → 4-(18-Methanesulfonyloxy-octadecyloxy)-benzoic acid methyl ester (59100-11-7)

Guidance literature:

With pyridine;

DOI:10.1021/jm00229a018

upstream raw materials:

4-(18-Hydroxy-octadecyloxy)-benzoic acid methyl ester

methanesulfonyl chloride

18-bromooctadecanoic acid

18-bromooctadecan-1-ol

Downstream raw materials:

4-(18-Mercapto-octadecyloxy)-benzoic acid

4-(18-Acetylsulfanyl-octadecyloxy)-benzoic acid methyl ester