C₂₇H₂₆ClN₇O₄S

Base Information

Chemical Name:C₂₇H₂₆ClN₇O₄S
CAS No.:1365992-76-2
Molecular Formula:C₂₇H₂₆ClN₇O₄S
Molecular Weight:580.067
Hs Code.:

C<sub>27</sub>H<sub>26</sub>ClN<sub>7</sub>O<sub>4</sub>S

Synonyms:C₂₇H₂₆ClN₇O₄S

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Chemical Property of C₂₇H₂₆ClN₇O₄S

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Technology Process of C₂₇H₂₆ClN₇O₄S

There total 12 articles about C₂₇H₂₆ClN₇O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148639-07-0
2-chloro-3-fluoro-4-iodopyridyne

: 1365992-76-2
C₂₇H₂₆ClN₇O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 1.5 h / Inert atmosphere; Reflux

2.1: thionyl chloride / 18 h / 100 °C / Inert atmosphere

3.1: thiourea; pyridine / isopropyl alcohol / 3 h / Inert atmosphere; Reflux

3.2: 1.5 h / Reflux

4.1: 1-methyl-pyrrolidin-2-one / 0.33 h / 150 °C

5.1: trimethylsilyl bromide / propiononitrile / 20 - 85 °C / Inert atmosphere

6.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 21 h / 80 °C / Inert atmosphere

With pyridine; thionyl chloride; trimethylsilyl bromide; caesium carbonate; thiourea; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; isopropyl alcohol; propiononitrile;

Reference yield:

: 17282-04-1
2-chloro-3-fluoropyridine

: 1365992-76-2
C₂₇H₂₆ClN₇O₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium diisopropyl amide / n-heptane; tetrahydrofuran; ethylbenzene / 4.67 h / -70 °C

1.2: 2 h / -70 - 20 °C

2.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 1.5 h / Inert atmosphere; Reflux

3.1: thionyl chloride / 18 h / 100 °C / Inert atmosphere

4.1: thiourea; pyridine / isopropyl alcohol / 3 h / Inert atmosphere; Reflux

4.2: 1.5 h / Reflux

5.1: 1-methyl-pyrrolidin-2-one / 0.33 h / 150 °C

6.1: trimethylsilyl bromide / propiononitrile / 20 - 85 °C / Inert atmosphere

7.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 21 h / 80 °C / Inert atmosphere

With pyridine; thionyl chloride; trimethylsilyl bromide; caesium carbonate; thiourea; lithium diisopropyl amide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; n-heptane; ethylbenzene; isopropyl alcohol; propiononitrile;

Reference yield:

: 354112-08-6
tert-butyl N-tert-butoxycarbonyl-N-(6-chloropyrimidin-4-yl)carbamate

: 1365992-76-2
C₂₇H₂₆ClN₇O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / 4 h / 70 °C

2: hydrogen / 5%-palladium/activated carbon / ethyl acetate; industrial methylated spirits / 18 h / 20 °C

3: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 21 h / 80 °C / Inert atmosphere

With sodium azide; hydrogen; caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 5%-palladium/activated carbon; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; industrial methylated spirits; ethyl acetate;