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((η5-C5(CH3)5)iron(carbonyl)2(tetrahydrofuran))(PF6)

Base Information
  • Chemical Name:((η5-C5(CH3)5)iron(carbonyl)2(tetrahydrofuran))(PF6)
  • CAS No.:89870-08-6
  • Molecular Formula:C16H23FeO3*F6P
  • Molecular Weight:464.168
  • Hs Code.:
((η5-C5(CH3)5)iron(carbonyl)2(tetrahydrofuran))(PF6)

Synonyms:((η5-C5(CH3)5)iron(carbonyl)2(tetrahydrofuran))(PF6)

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Chemical Property of ((η5-C5(CH3)5)iron(carbonyl)2(tetrahydrofuran))(PF6)
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Technology Process of ((η5-C5(CH3)5)iron(carbonyl)2(tetrahydrofuran))(PF6)

There total 1 articles about ((η5-C5(CH3)5)iron(carbonyl)2(tetrahydrofuran))(PF6) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In tetrahydrofuran; dichloromethane; stirring a soln. of Fe-complex and ((C5H5)2Fe)PF6 in CH2Cl2 and THF at room temp. for 20 h under N2; removal of solvents, transferring to a frit, washing repeatedly with deoxygenated ether to remove ferrocene, drying;
DOI:10.1016/0022-328X(93)83287-6
Guidance literature:
With triphenylphosphine; In dichloromethane; addn. of PPh3 (excess 3/1) to CH2Cl2 soln. of educt at room temp.; 12 h; recrystn. from acetone or ethanol;
DOI:10.1016/0022-328X(84)80118-7
Guidance literature:
In dichloromethane; addn. of P(OPh)3 (excess 3/1) to CH2Cl2 soln. of educt at room temp.; 12 h; recrystn. from acetone or ethanol;
DOI:10.1016/0022-328X(84)80118-7
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