1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate

Base Information

• Chemical Name: 1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate
• CAS No.: 931096-02-5
• Molecular Formula: C₃₁H₃₃NO₇
• Molecular Weight: 531.606

Synonyms:1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate

Chemical Property of 1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Technology Process of 1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate

There total 3 articles about 1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-tert-butyl 2,2-dibenzyl 1-(phenylamino)ethane-1,2,2-tricarboxylate (931095-95-3) + acetyl chloride (75-36-5) → 1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate (931096-02-5)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1016/j.tet.2006.12.058

Reference yield:

1,1-dibenzyl 2-tert-butyl ethenetricarboxylate (811418-53-8) → 1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate (931096-02-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / ZnCl₂ / CH₂Cl₂ / 20 °C

2: 72 percent / Et₃N / CH₂Cl₂ / 16 h / 20 °C

With triethylamine; zinc(II) chloride; In dichloromethane;

DOI:10.1016/j.tet.2006.12.058

Reference yield:

aniline (62-53-3) → 1-tert-butyl 2,2-dibenzyl 1-(acetylphenylamino)ethane-1,2,2-tricarboxylate (931096-02-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / ZnCl₂ / CH₂Cl₂ / 20 °C

2: 72 percent / Et₃N / CH₂Cl₂ / 16 h / 20 °C

With triethylamine; zinc(II) chloride; In dichloromethane;

DOI:10.1016/j.tet.2006.12.058

upstream raw materials:

1-tert-butyl 2,2-dibenzyl 1-(phenylamino)ethane-1,2,2-tricarboxylate

acetyl chloride

1,1-dibenzyl 2-tert-butyl ethenetricarboxylate

aniline

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