(3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol

Base Information

Chemical Name:(3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol
CAS No.:98362-10-8
Molecular Formula:C₁₁H₁₉NO₃
Molecular Weight:213.277
Hs Code.:

Synonyms:(3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol

Suppliers and Price of (3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol

Chemical Property:

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Technology Process of (3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol

There total 1 articles about (3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 98361-98-9,98362-12-0,107025-31-0
(E)-3-((2R,3S)-3-{(4R,5R)-2,2-Dimethyl-5-[(2,2,2-trifluoro-acetylamino)-methyl]-[1,3]dioxolan-4-yl}-oxiranyl)-acrylic acid ethyl ester

: 85624-09-5
(3aR,9R,9aR,9bS)-octahydro-2,2-dimethyl-[1,3]dioxolo[4,5-a]indolizin-9-ol

: 98362-10-8
(3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; ethanol; Heating;
DOI:10.1021/jo00220a063

Reference yield:

: 98362-10-8
(3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol

: 72741-87-8
swainsonine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / 5 °C

2: dimethylformamide / 100 °C

3: 1.) MeONa, 2.) trifluoroacetic acid / 1.) MeOH, r.t., 2.) H₂O, r.t.

With sodium methylate; trifluoroacetic acid; In pyridine; N,N-dimethyl-formamide;

Reference yield:

: 98362-10-8
(3aR,8aS,9S,9aS)-2,2-Dimethyl-octahydro-[1,3]dioxolo[4,5-f]indolizin-9-ol

: 107794-67-2
Benzoic acid (3aR,9R,9aR,9bS)-2,2-dimethyl-octahydro-[1,3]dioxolo[4,5-a]indolizin-9-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / 5 °C

2: dimethylformamide / 100 °C

In pyridine; N,N-dimethyl-formamide;