(E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate

Base Information

Chemical Name:(E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate
CAS No.:1451153-21-1
Molecular Formula:C₂₅H₂₆F₃NO₄S
Molecular Weight:493.547
Hs Code.:

Synonyms:(E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate

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Chemical Property of (E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate

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Technology Process of (E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate

There total 1 articles about (E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 124070-44-6
4-methyl-N-(1-phenylhept-2-yn-1-yl)benzenesulfonamide

: 70577-95-6
methyl 4,4,4-trifluoro-2-butynoate

: 1451153-21-1
(E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate

Guidance literature:: With caesium carbonate; In dichloromethane; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ol4020738

Reference yield: 88.0%

: 1451153-21-1
(E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate

: 1451153-44-8
(E)-methyl 3-benzylidene-4-(4-methylphenylsulfonamido)-2-(n-butyl)-4-(trifluoromethyl)cyclobut-1-enecarboxylate

Guidance literature:: In 1,4-dioxane; at 100 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol4020738

Reference yield: 51.0%

: 1451153-21-1
(E)-methyl 4,4,4-trifluoro-3-(4-methyl-N-(1-phenylhept-2-yn-1-yl)phenylsulfonamido)but-2-enoate

: methyl 3-phenyl-6-propyl-4-tosyl-1-(trifluoromethyl)-2-azabicyclo[3.2.0]hept-2-ene-7-carboxylate

Guidance literature:: With caesium carbonate; In dimethyl sulfoxide; at 100 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.5b01474