C₁₆H₂₀O₅

Base Information

Chemical Name:C₁₆H₂₀O₅
CAS No.:1264833-25-1
Molecular Formula:C₁₆H₂₀O₅
Molecular Weight:292.332
Hs Code.:

C<sub>16</sub>H<sub>20</sub>O<sub>5</sub>

Synonyms:C₁₆H₂₀O₅

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Chemical Property of C₁₆H₂₀O₅

Chemical Property:

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Technology Process of C₁₆H₂₀O₅

There total 9 articles about C₁₆H₂₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₂₄H₂₈O₆

: 1264833-25-1
C₁₆H₂₀O₅

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja1103102

Reference yield:

: 1264833-09-1
C₉H₁₆O₄

: 98-88-4
benzoyl chloride

: C₁₆H₂₀O₅

: 1264833-25-1
C₁₆H₂₀O₅

Guidance literature:: C₉H₁₆O₄; With 2,6-bis((S)-3,3-dibutyl-2-phenyl-3,4-dihydro-2H-pyrrol-5-yl)pyridine; copper dichloride; In dichloromethane; at 20 ℃; Inert atmosphere;

benzoyl chloride; With triethylamine; In dichloromethane; at -78 ℃; for 12h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja1103102

Reference yield:

: 1264833-22-8
C₁₃H₁₆O₃

: 1264833-25-1
C₁₆H₂₀O₅

Guidance literature:: Multi-step reaction with 4 steps

1: (+/-)-camphorsulfonic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

2: sodium periodate; osmium(VIII) oxide; water / 1,4-dioxane / 6 h / 0 - 20 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

4: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; water; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; dichloromethane; mineral oil;
DOI:10.1021/ja1103102