3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole

Base Information

Chemical Name:3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole
CAS No.:1221717-28-7
Molecular Formula:C₁₈H₁₉N₃O₅
Molecular Weight:357.366
Hs Code.:

Synonyms:3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole

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Chemical Property of 3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole

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Technology Process of 3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole

There total 4 articles about 3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1257321-31-5
3-hydroxy-4-methoxybenzenecarboximidoyl chloride

: 3291-03-0
3,4,5-trimethoxybenzohydrazide

: 1221717-28-7
3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole

Guidance literature:: With sodium methylate; In methanol; at 45 ℃; Reflux;
DOI:10.1021/np1004278

Reference yield:

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 1221717-28-7
3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 6 h / Reflux

2: sodium methylate / methanol / 45 °C / Reflux

With sodium methylate; hydrazine hydrate; In methanol;
DOI:10.1021/np1004278

Reference yield:

: 52805-46-6
2-methoxy-5-cyanophenol

: 1221717-28-7
3-(3-hydroxy-4-methoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; methanol / diethyl ether / 0 - 5 °C

2: sodium methylate / methanol / 45 °C / Reflux

With hydrogenchloride; methanol; sodium methylate; In methanol; diethyl ether;
DOI:10.1021/np1004278