9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N⁶-benzoyladenine

Base Information

• Chemical Name: 9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N⁶-benzoyladenine
• CAS No.: 1042664-98-1
• Molecular Formula: C₃₅H₅₁F₃N₆O₈Si₂
• Molecular Weight: 796.992

Synonyms:9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N⁶-benzoyladenine

Chemical Property of 9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N⁶-benzoyladenine

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Technology Process of 9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N⁶-benzoyladenine

There total 1 articles about 9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N⁶-benzoyladenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}adenine (1042665-26-8) + benzoyl chloride (98-88-4) → 9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N6-benzoyladenine (1042664-98-1)

Guidance literature:

With pyridine; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2008.04.110

Reference yield: 86.0%

9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N6-benzoyladenine (1042664-98-1) → 9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-β-D-ribofuranosyl}-N6-benzoyladenine (1042665-09-7)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.166667h;

DOI:10.1016/j.tet.2008.04.110

upstream raw materials:

9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}adenine

benzoyl chloride

Downstream raw materials:

9-{2-O-[(3-(2,2,2-trifluoroacetamido)propoxy)methyl]-β-D-ribofuranosyl}-N⁶-benzoyladenine

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