C₁₈H₃₀O₂Si

Base Information

Chemical Name:C₁₈H₃₀O₂Si
CAS No.:1622087-78-8
Molecular Formula:C₁₈H₃₀O₂Si
Molecular Weight:306.521
Hs Code.:

C<sub>18</sub>H<sub>30</sub>O<sub>2</sub>Si

Synonyms:C₁₈H₃₀O₂Si

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Chemical Property of C₁₈H₃₀O₂Si

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Technology Process of C₁₈H₃₀O₂Si

There total 1 articles about C₁₈H₃₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 994-30-9
triethylsilyl chloride

: 88981-35-5
(2S)-1-(benzyloxy)pent-4-en-2-ol

: 1622087-78-8
C₁₈H₃₀O₂Si

Guidance literature:: (2S)-1-(benzyloxy)pent-4-en-2-ol; With triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;

triethylsilyl chloride; With dmap; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/acs.joc.1c00686

Reference yield: 67.0%

: 2021-28-5
ethyl dihydrocinnamate

: 1622087-78-8
C₁₈H₃₀O₂Si

: 1622087-58-4
C₂₇H₄₀O₃Si

Guidance literature:: With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/ejoc.201402175

Reference yield:

: 1622087-78-8
C₁₈H₃₀O₂Si

: C₁₆H₂₀O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; tert-butyl alcohol; water / 12 h / 0 - 20 °C

2.1: sodium hydrogencarbonate; sodium periodate / tetrahydrofuran; water / 0 - 20 °C

3.1: potassium hexamethylsilazane / tetrahydrofuran / -78 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: camphor-10-sulfonic acid / dichloromethane; methanol / 0 °C

5.1: triethylamine; dmap / dichloromethane / 1 h / 0 °C / Inert atmosphere

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; tert-butyl alcohol; water / 12 h / 0 - 20 °C

6.2: 6 h

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

With dmap; sodium periodate; osmium(VIII) oxide; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/acs.joc.1c00686