(2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran

Base Information

Chemical Name:(2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran
CAS No.:212395-01-2
Molecular Formula:C₃₂H₃₆O₅
Molecular Weight:500.635
Hs Code.:

Synonyms:(2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran

Suppliers and Price of (2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran

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Chemical Property of (2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran

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Technology Process of (2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran

There total 3 articles about (2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 109-92-2,25104-37-4
ethyl vinyl ether

: 161275-25-8
3-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-1-propene

: 212395-01-2
(2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran

Guidance literature:: With mercury(II) diacetate;
DOI:10.1021/jo980996k

Reference yield: 28.0%

: 212395-00-1
Formic acid (2S,3S,4S,5R,6R)-2-allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl ester

: 74-95-3
1,1-dibromomethane

: 200621-47-2
(4S,5R,6S,7S,8R)-1,2-anhydro-6,7,9-tribenzyloxypyrano<4,5>pyran

: 212395-01-2
(2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran

Guidance literature:: With titanium tetrachloride; lead(II) chloride; zinc; Yields of byproduct given;
DOI:10.1021/jo980996k

Reference yield:

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 212395-01-2
(2S,3S,4S,5R,6R)-2-Allyl-4,5-bis-benzyloxy-6-benzyloxymethyl-3-vinyloxy-tetrahydro-pyran

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dimethyldioxirane / 1.) CH₂Cl₂, 2.) THF, 0 deg C

2: 58 percent / Hg(OAc)2

With mercury(II) diacetate; 3,3-dimethyldioxirane;
DOI:10.1021/jo980996k