2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt

Base Information

Chemical Name:2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt
CAS No.:1310709-72-8
Molecular Formula:C₁₈H₂₄NO₈*Li
Molecular Weight:389.331
Hs Code.:

Synonyms:2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt

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Chemical Property of 2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt

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Technology Process of 2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt

There total 4 articles about 2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1310709-63-7
2-(α-D-C-mannopyranosyl)-(S)-N-benzoylvaline methyl ester

: 1310709-72-8
2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt

Guidance literature:: With lithium hydroxide monohydrate; In water; for 3h;
DOI:10.1021/jo2002962

Reference yield:

: 2873-29-2
D-glucal triacetate

: 1310709-72-8
2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; hydroquinone / 1 h / Darkness; Heating

1.2: 0.5 h

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; triethylamine / tetrahydrofuran / 2 h / 20 °C / Molecular sieve

3.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 24 h / 20 °C / Inert atmosphere

4.1: sodium methylate / methanol / 20 °C / Inert atmosphere

4.2: Inert atmosphere

5.1: lithium hydroxide monohydrate / water / 3 h

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; osmium(VIII) oxide; lithium hydroxide monohydrate; water; sodium methylate; 4-methylmorpholine N-oxide; (1R,2R)-1,2-bis[(2-diphenylphosphanyl)benzoylamino]cyclohexane; triethylamine; hydroquinone; In tetrahydrofuran; methanol; water; acetone; tert-butyl alcohol;
DOI:10.1021/jo2002962

Reference yield:

: 1310709-60-4
2-(4',6'-di-O-acetyl-α-D-mannopyranosyl)-2-benzamido-(2S)-3-methylbutanoic acid 1',2'-lactone

: 1310709-72-8
2-α-D-mannopyranosyl-2-benzamido-(2S)-3-methylbutanoic acid lithium salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: lithium hydroxide monohydrate / water / 3 h

With lithium hydroxide monohydrate; sodium methylate; In methanol; water;
DOI:10.1021/jo2002962