5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

Base Information

Chemical Name:5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione
CAS No.:1372400-60-6
Molecular Formula:C₂₇H₂₆O₅
Molecular Weight:430.5
Hs Code.:

Synonyms:5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

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Chemical Property of 5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

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Technology Process of 5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

There total 3 articles about 5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1352708-12-3
trimethyl((5-methyl-2-(o-tolyl)-1,3,2-dioxaborinan-5-yl)methoxy)silane

: 666698-12-0
C₂₀H₁₈O₅

: 1372400-60-6
5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide; In 1,4-dioxane; at 20 ℃;
DOI:10.1039/c1ob06586f

Reference yield:

: C₁₂H₁₇BO₃

: 1372400-60-6
5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

2: chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide / 1,4-dioxane / 20 °C

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triethylamine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1039/c1ob06586f

Reference yield:

: 16419-60-6
2-Methylphenylboronic acid

: 1372400-60-6
5-((2-(benzyloxy)phenyl)(o-tolyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 3 h

2: triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

3: chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide / 1,4-dioxane / 20 °C

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triethylamine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; toluene;
DOI:10.1039/c1ob06586f