(2,3-Dihydro-3-methyl-1H-indol-1-yl)phenylmethanone

Base Information

Chemical Name:(2,3-Dihydro-3-methyl-1H-indol-1-yl)phenylmethanone
CAS No.:21874-23-7
Molecular Formula:C₁₆H₁₅NO
Molecular Weight:237.301
Hs Code.:
DSSTox Substance ID:DTXSID301223767
Nikkaji Number:J856.510D

Synonyms:DTXSID301223767;21874-23-7;(2,3-Dihydro-3-methyl-1H-indol-1-yl)phenylmethanone

Suppliers and Price of (2,3-Dihydro-3-methyl-1H-indol-1-yl)phenylmethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2,3-Dihydro-3-methyl-1H-indol-1-yl)phenylmethanone

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:237.115364102
Heavy Atom Count:18
Complexity:308

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1CN(C2=CC=CC=C12)C(=O)C3=CC=CC=C3

Technology Process of (2,3-Dihydro-3-methyl-1H-indol-1-yl)phenylmethanone

There total 7 articles about (2,3-Dihydro-3-methyl-1H-indol-1-yl)phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.1%

: 4375-15-9
3-methyl-2,3-dihydro-1H-indole

: 98-88-4
benzoyl chloride

: 21874-23-7
(3-methylindolin-1-yl)(phenyl)methanone

Guidance literature:: With sodium hydroxide;

Reference yield: 66.0%

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 73396-91-5
2-bromo-N-(prop-2-enyl)aniline

: 21874-23-7
(3-methylindolin-1-yl)(phenyl)methanone

Guidance literature:: 2-bromo-N-(prop-2-enyl)aniline; With tert.-butyl lithium; In diethyl ether; n-heptane; at -78 ℃; for 1h;

With N,N,N,N,-tetramethylethylenediamine; In diethyl ether; n-heptane; at 5 ℃; for 2h;

benzoic acid ethyl ester; With ethanol; In diethyl ether; n-heptane; at 20 ℃; for 1h;
DOI:10.1016/S0040-4039(03)01204-8

Reference yield:

: 119488-08-3
N-allyl benz(o-bromo)anilide

: 21874-23-7
(3-methylindolin-1-yl)(phenyl)methanone

: 119488-15-2
5,6-dihydro-6-oxo-N-allylphenanthridine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2h; Yield given. Yields of byproduct given; Heating;
DOI:10.1039/a607060d