diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate

Base Information

Chemical Name:diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate
CAS No.:1404216-18-7
Molecular Formula:C₂₁H₃₉O₅PSi
Molecular Weight:430.597
Hs Code.:

Synonyms:diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate

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Chemical Property of diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate

Chemical Property:

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Technology Process of diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate

There total 4 articles about diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1404216-17-6
[3-(benzyloxy)-2-(bromomethyl)propoxy](tert-butyl)dimethylsilane

: 122-52-1
triethyl phosphite

: 1404216-18-7
diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate

Guidance literature:: at 175 ℃; for 18h;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1404216-18-7
diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Cooling with ice

1.2: 2 h

2.1: carbon tetrabromide; triphenylphosphine; pyridine / dichloromethane / 2.5 h / Inert atmosphere

3.1: 18 h / 175 °C

With pyridine; carbon tetrabromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; mineral oil;

Reference yield:

: 117087-18-0
2-((benzyloxy)methyl)propane-1,3-diol

: 1404216-18-7
diethyl {2-[(benzyloxy)methyl]-3-[(tert-butyldimethylsilyl)oxy]propyl}phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C / Cooling with ice

1.2: 2 h

2.1: carbon tetrabromide; triphenylphosphine; pyridine / dichloromethane / 2.5 h / Inert atmosphere

3.1: 18 h / 175 °C

With pyridine; carbon tetrabromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; mineral oil;