methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate

Base Information

Chemical Name:methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate
CAS No.:300719-62-4
Molecular Formula:C₁₈H₂₀O₅
Molecular Weight:317.343
Hs Code.:

methyl 2-benzyloxymethoxy-4-[O<sub>13</sub>CH<sub>3</sub>]-methoxy-6-methyl benzoate

Synonyms:methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate

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Chemical Property of methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate

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Technology Process of methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate

There total 2 articles about methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3587-60-8
Benzyloxymethyl chloride

: 300719-64-6
Methyl 2-hydroxy-4-[13C]methoxy-6-methylbenzoate

: 300719-62-4
methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate

Guidance literature:: Methyl 2-hydroxy-4-[13C]methoxy-6-methylbenzoate; With sodium methylate; In methanol;

Benzyloxymethyl chloride; With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1039/b003053h

Reference yield:

: 3187-58-4
methyl orsellinate

: 300719-62-4
methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 91 percent / K₂CO₃ / acetone / 3 h / Heating

2.1: NaOMe / methanol

2.2: 85 percent / Et₃N / tetrahydrofuran / 12 h / 20 °C

With sodium methylate; potassium carbonate; In methanol; acetone; 1.1: Methylation / 2.1: Metallation / 2.2: Etherification;
DOI:10.1039/b003053h

Reference yield: 36.0%

: 300719-37-3
(R)-5-(tert-Butyldimethylsilyloxy)-3-methoxy-5-methylhex-2-en-1-one

: 300719-62-4
methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate

: 300719-58-8
(R)-8-Benzyloxymethoxy-3-(tert-butyldimethylsilyloxy)-9-hydroxy-6-[13C]methoxy-3-methyl-3,4-dihydroanthracen-1(2H)-one

Guidance literature:: methyl 2-benzyloxymethoxy-4-[O₁₃CH₃]-methoxy-6-methyl benzoate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

(R)-5-(tert-Butyldimethylsilyloxy)-3-methoxy-5-methylhex-2-en-1-one; In tetrahydrofuran; hexane; at -70 - 20 ℃; for 0.75h;
DOI:10.1039/b003053h