(Z)-1,1-dimethyl-2-[phenyl(trimethylsilyl)methylene]-3,4-dipropyl-1,2-dihydrosilete

Base Information

Chemical Name:(Z)-1,1-dimethyl-2-[phenyl(trimethylsilyl)methylene]-3,4-dipropyl-1,2-dihydrosilete
CAS No.:1370259-44-1
Molecular Formula:C₂₁H₃₄Si₂
Molecular Weight:342.672
Hs Code.:

Synonyms:(Z)-1,1-dimethyl-2-[phenyl(trimethylsilyl)methylene]-3,4-dipropyl-1,2-dihydrosilete

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1,1-dimethyl-2-[phenyl(trimethylsilyl)methylene]-3,4-dipropyl-1,2-dihydrosilete

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Technology Process of (Z)-1,1-dimethyl-2-[phenyl(trimethylsilyl)methylene]-3,4-dipropyl-1,2-dihydrosilete

There total 2 articles about (Z)-1,1-dimethyl-2-[phenyl(trimethylsilyl)methylene]-3,4-dipropyl-1,2-dihydrosilete which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: (Z)-1,1,1,2,2-pentamethyl-2-[5-(2-phenylethynyl)oct-4-en-4-yl]disilane

: 1370259-44-1
(Z)-1,1-dimethyl-2-[phenyl(trimethylsilyl)methylene]-3,4-dipropyl-1,2-dihydrosilete

Guidance literature:: With di(rhodium)tetracarbonyl dichloride; In toluene; at 110 ℃; for 4.5h; Inert atmosphere;
DOI:10.1039/c2ob25242b

Reference yield:

: 1560-28-7
pentamethylchlorodisilane

: 1231255-92-7
(Z)-(4-bromo-3-propylhept-3-en-1-yn-1-yl)benzene

: 1370259-44-1
(Z)-1,1-dimethyl-2-[phenyl(trimethylsilyl)methylene]-3,4-dipropyl-1,2-dihydrosilete

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / Inert atmosphere

2: di(rhodium)tetracarbonyl dichloride / toluene / 4.5 h / 110 °C / Inert atmosphere

With n-butyllithium; di(rhodium)tetracarbonyl dichloride; In toluene;
DOI:10.1039/c2ob25242b