2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen

Base Information

• Chemical Name: 2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen
• CAS No.: 71959-45-0
• Molecular Formula: C₁₆H₁₆O₄S₂
• Molecular Weight: 336.433
• Mol file: 71959-45-0.mol

Synonyms:2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen

Chemical Property of 2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen

There total 2 articles about 2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

allyl dithiobenzoate (27249-64-5) + dimethyl acetylenedicarboxylate (762-42-5) → 2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen (71959-45-0)

Guidance literature:

for 168h; Ambient temperature;

Reference yield:

→ 2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen (71959-45-0)

Guidance literature:

Dithiobenzoat (Ib), Ester (II);

Reference yield:

2-Phenyl-2-allyl-4,5-dimethoxycarbonyl-1,3-dithiolen (71959-45-0) → 1-butylbenzene (104-51-8) + Dimethyl succinate (106-65-0)

Guidance literature:

With nickel; In methanol; for 6h; Product distribution; Heating;

upstream raw materials:

allyl dithiobenzoate

dimethyl acetylenedicarboxylate

Downstream raw materials:

1-butylbenzene

Dimethyl succinate