Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester

Base Information

Chemical Name:Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester
CAS No.:1046453-74-0
Molecular Formula:C₁₉H₂₆N₂O₁₀
Molecular Weight:442.423
Hs Code.:

Synonyms:Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester

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Chemical Property of Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester

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Technology Process of Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester

There total 3 articles about Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1202249-74-8
1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate

: 20379-60-6
α-D-Glucopyranosyl azide

: 1046453-74-0
Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester

: C₁₉H₂₆N₂O₁₀

Guidance literature:: 1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate; α-D-Glucopyranosyl azide; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 20 - 40 ℃; Inert atmosphere;

With water; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 40 ℃; for 2h;
DOI:10.1002/ejoc.200900692

Reference yield: 35.0%

: 20379-60-6
α-D-Glucopyranosyl azide

: 848863-20-7
N-benzyloxycarbonyl-L-aspartic acid 4-(2-diphenylphosphanyl-phenyl) ester 1-methyl ester

: 1046453-74-0
Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester

Guidance literature:: α-D-Glucopyranosyl azide; N-benzyloxycarbonyl-L-aspartic acid 4-(2-diphenylphosphanyl-phenyl) ester 1-methyl ester; In N,N-dimethyl acetamide; at 50 ℃; for 0.833333h; microwave irradiation;

With water; In N,N-dimethyl acetamide; at 50 ℃; for 0.833333h; Further stages.; microwave irradiation;
DOI:10.1016/j.carres.2008.04.023

Reference yield: 25.0%

: 20379-60-6
α-D-Glucopyranosyl azide

: 848863-20-7
N-benzyloxycarbonyl-L-aspartic acid 4-(2-diphenylphosphanyl-phenyl) ester 1-methyl ester

: C₁₉H₂₆N₂O₁₀

: 1046453-74-0
Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-asparagine-O-methyl ester

Guidance literature:: α-D-Glucopyranosyl azide; N-benzyloxycarbonyl-L-aspartic acid 4-(2-diphenylphosphanyl-phenyl) ester 1-methyl ester; In N,N-dimethyl acetamide; at 40 ℃; for 4h;

With water; In N,N-dimethyl acetamide; at 40 ℃; for 2h; Further stages.;
DOI:10.1016/j.carres.2008.04.023