1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate

Base Information

Chemical Name:1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate
CAS No.:1202249-74-8
Molecular Formula:C₃₁H₂₇FNO₆P
Molecular Weight:559.531
Hs Code.:

Synonyms:1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate

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Chemical Property of 1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate

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Technology Process of 1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate

There total 1 articles about 1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4668-42-2
(S)-2-benzyloxycarbonylamino-succinic acid 1-methyl ester

: 2-(diphenylphosphanyl)-4-fluorophenol

: 1202249-74-8
1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.200900692

Reference yield: 77.0%

: 20379-59-3
D-glucopyranosyl azide

: 1202249-74-8
1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate

: 1046453-80-8
Nα-(benzyloxycarbonyl)-Nγ-(β-D-glucopyranosyl)-L-asparagine O-methyl ester

Guidance literature:: D-glucopyranosyl azide; 1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 20 - 40 ℃; Inert atmosphere;

With water; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 40 ℃; for 2h;
DOI:10.1002/ejoc.200900692

Reference yield: 74.0%

: 35899-89-9
1-amido-1-deoxygalactopyranose

: 1202249-74-8
1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate

: 1202249-83-9
Nα-(benzyloxycarbonyl)-Nγ-(β-D-galactopyranosyl)-L-asparagine O-methyl ester

Guidance literature:: 1-amido-1-deoxygalactopyranose; 1-methyl 4-[2-(diphenylphosphanyl)-4-fluorophenyl] N-(benzyloxycarbonyl)-L-aspartate; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 20 - 40 ℃; Inert atmosphere;

With water; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; N,N-dimethyl acetamide; at 40 ℃; for 2h;
DOI:10.1002/ejoc.200900692