1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate

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Chemical Name:1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate
CAS No.:913622-36-3
Molecular Formula:C₂₁H₂₆INO₉
Molecular Weight:563.343
Hs Code.:

Synonyms:1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate

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Chemical Property of 1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate

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Technology Process of 1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate

There total 7 articles about 1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 913622-34-1
1-(2-methoxy-3,6-bis(methoxymethoxy)-5-nitrophenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate

: 913622-36-3
1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate

Guidance literature:: With sodium tetrahydroborate; tin(ll) chloride; In ethanol; for 0.333333h; Heating;
DOI:10.1021/jo061054f

Reference yield:

: 854261-02-2
1-(2-methoxy-3,6-bis(methoxymethoxy)phenyl)propan-2-ol

: 913622-36-3
1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: NH₄NO₃; (CF₃CO)2O / acetonitrile / 0.25 h / 20 °C

1.2: LiOH / tetrahydrofuran; methanol; H₂O / 0.08 h

2.1: 52 percent / DMAP; DCC / dimethylformamide; tetrahydrofuran / 12 h / 50 °C

3.1: 63 percent / SnCl₂*H₂O; NaBH₄ / ethanol / 0.33 h / Heating

With ammonium nitrate; dmap; sodium tetrahydroborate; dicyclohexyl-carbodiimide; trifluoroacetic anhydride; tin(ll) chloride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo061054f

Reference yield:

: 854261-03-3
1-(2-methoxy-3,6-bis(methoxymethoxy)-5-nitrophenyl)propan-2-ol

: 913622-36-3
1-(3-amino-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-iodo-2,4-dihydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / DMAP; DCC / dimethylformamide; tetrahydrofuran / 12 h / 50 °C

2: 63 percent / SnCl₂*H₂O; NaBH₄ / ethanol / 0.33 h / Heating

With dmap; sodium tetrahydroborate; dicyclohexyl-carbodiimide; tin(ll) chloride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo061054f