(2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal

Base Information

Chemical Name:(2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal
CAS No.:219931-69-8
Molecular Formula:C₂₃H₃₄N₂O₇S₂
Molecular Weight:514.664
Hs Code.:

Synonyms:(2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal

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Chemical Property of (2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal

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Technology Process of (2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal

There total 6 articles about (2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105089-88-1
(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrole

: 4-(4-chlorocarbonyl-2-methoxy-5-nitro-phenoxy)-butyric acid ethyl ester

: 219931-69-8
(2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo9812072

Reference yield:

: 219931-67-6
ethyl 4-(4-formyl-2-methoxy-5-nitrophenoxy)butanoate

: 219931-69-8
(2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: aq. sodium chlorite; sulfamic acid

2: SO₂Cl₂ / benzene / 2 h / 20 °C

3: Et₃N / CH₂Cl₂ / 1 h / 0 °C

With sodium chlorite; sulfuryl dichloride; aminosulfonic acid; triethylamine; In dichloromethane; benzene;
DOI:10.1515/HC.2002.8.1.19

Reference yield:

: 219931-68-7
5-methoxy-4-[3-(carbethoxy)propyloxy]-2-nitrobenzoic acid

: 219931-69-8
(2S)-N-[5-methoxy-4-[3-(carboethoxy)propyloxy]-2-nitrobenzoyl]pyrrolidine-2-carboxaldehydediethylthioacetal

Guidance literature:: Multi-step reaction with 2 steps

1: SO₂Cl₂ / benzene / 2 h / 20 °C

2: Et₃N / CH₂Cl₂ / 1 h / 0 °C

With sulfuryl dichloride; triethylamine; In dichloromethane; benzene;
DOI:10.1515/HC.2002.8.1.19