N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide

Base Information

Chemical Name:N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide
CAS No.:96866-08-9
Molecular Formula:C₂₄H₃₁N₃O₄
Molecular Weight:425.528
Hs Code.:

Synonyms:N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide

Chemical Property:

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Technology Process of N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide

There total 5 articles about N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 67681-99-6
α-[(benzyloxy)carbamoyl]hydrocinnamic acid

: 87429-14-9
glycine isopentylamide trifluoroacetate

: 96866-08-9
N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide

Guidance literature:: With N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; benzotriazol-1-ol; triethylamine; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield:

: 2985-39-9,175521-78-5
2-benzylmalonic acid monoethyl ester

: 96866-08-9
N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Et₃N, 1-hydroxybenzotriazole (HOBt), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

2: 64 percent / 2.5 N aq. NaOH / methanol / 4 h / Ambient temperature

3: 88 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), N-cyclohexyl-N'-<2-(4-morpholinyl)ethyl>carbodiimide methol p-toluenosulfonate / tetrahydrofuran / Ambient temperature

With sodium hydroxide; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/jm00147a007

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 96866-08-9
N-<2(RS)-<<(benzyloxy)amino>carbonyl>-1-oxo-3-phenylpropyl>glycine isopentylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Et₃N, 1-hydroxybenzotriazole (HOBt), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

2: 64 percent / 2.5 N aq. NaOH / methanol / 4 h / Ambient temperature

3: 88 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), N-cyclohexyl-N'-<2-(4-morpholinyl)ethyl>carbodiimide methol p-toluenosulfonate / tetrahydrofuran / Ambient temperature

With sodium hydroxide; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/jm00147a007