Technology Process of C38H48O15
There total 7 articles about C38H48O15 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
at 5 - 20 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridine / chloroform / 6 h / 0 - 20 °C
2.1: hydrogen bromide; acetic acid / chloroform / 0 - 20 °C
3.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere
3.2: 16 h / 20 °C / Cooling with ice-salt bath
4.1: sodium methylate; methanol / chloroform / 1 h / 20 °C / Inert atmosphere
5.1: pyridine / 20 h / 5 - 20 °C
With
pyridine; methanol; hydrogen bromide; sodium methylate; acetic acid;
In
dichloromethane; chloroform;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen bromide; acetic acid / chloroform / 0 - 20 °C
2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere
2.2: 16 h / 20 °C / Cooling with ice-salt bath
3.1: sodium methylate; methanol / chloroform / 1 h / 20 °C / Inert atmosphere
4.1: pyridine / 20 h / 5 - 20 °C
With
pyridine; methanol; hydrogen bromide; sodium methylate; acetic acid;
In
dichloromethane; chloroform;