1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone

Base Information

Chemical Name:1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone
CAS No.:345300-15-4
Molecular Formula:C₁₉H₂₉NO₄
Molecular Weight:335.444
Hs Code.:

Synonyms:1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone

Chemical Property:

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Technology Process of 1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone

There total 4 articles about 1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38031-78-6
3-tert-butylpyridine

: 345300-15-4
1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / benzene / 48 h / Ambient temperature

2: 1.) hydrogen, 2.) NaBH₄, 2 N aq. NaOH / 1.) Pt / 1.) ethanol, 25 deg C, 15 h, 2.) ethanol, rt

3: mercuric acetate-ethylenediaminetetraacetic acid / aq. acetic acid / 1.5 h / Heating

With sodium hydroxide; sodium tetrahydroborate; ethylenediaminetetraacetic acid; mercury(II) diacetate; hydrogen; platinum; In acetic acid; benzene;
DOI:10.1248/cpb.29.2691

Reference yield:

: 1835-02-5
2-Bromo-1-(3,4-dimethoxyphenyl)ethanone

: 345300-15-4
1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / benzene / 48 h / Ambient temperature

2: 1.) hydrogen, 2.) NaBH₄, 2 N aq. NaOH / 1.) Pt / 1.) ethanol, 25 deg C, 15 h, 2.) ethanol, rt

3: mercuric acetate-ethylenediaminetetraacetic acid / aq. acetic acid / 1.5 h / Heating

With sodium hydroxide; sodium tetrahydroborate; ethylenediaminetetraacetic acid; mercury(II) diacetate; hydrogen; platinum; In acetic acid; benzene;
DOI:10.1248/cpb.29.2691

Reference yield:

: 80426-69-3
1-(3,4-dimethoxyphenacyl)-3-(1,1-dimethylethyl)pyridinium bromide

: 345300-15-4
1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen, 2.) NaBH₄, 2 N aq. NaOH / 1.) Pt / 1.) ethanol, 25 deg C, 15 h, 2.) ethanol, rt

2: mercuric acetate-ethylenediaminetetraacetic acid / aq. acetic acid / 1.5 h / Heating

With sodium hydroxide; sodium tetrahydroborate; ethylenediaminetetraacetic acid; mercury(II) diacetate; hydrogen; platinum; In acetic acid;
DOI:10.1248/cpb.29.2691