diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate

Base Information

Chemical Name:diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate
CAS No.:1316240-10-4
Molecular Formula:C₂₂H₁₉O₄P
Molecular Weight:378.364
Hs Code.:

Synonyms:diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate

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Chemical Property of diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate

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Technology Process of diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate

There total 4 articles about diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1316239-77-6
(Z)-2-iodo-1-phenylvinyl diphenyl phosphate

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1316240-10-4
diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 20 ℃; for 6h; stereoselective reaction;
DOI:10.1039/c1cc12052b

Reference yield: 68.0%

: 1316239-77-6
(Z)-2-iodo-1-phenylvinyl diphenyl phosphate

: 75927-49-0
pinacol vinylboronate

: 1316240-10-4
diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphate potassium salt; In 1,4-dioxane; stereoselective reaction;
DOI:10.1039/c1cc12052b

Reference yield:

: 838-85-7
diphenyl hydrogen phosphate

: 1316240-10-4
diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate / toluene / 4 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphate potassium salt / 1,4-dioxane

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphate potassium salt; (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; In 1,4-dioxane; toluene;
DOI:10.1039/c1cc12052b