1-((Z)-deca-1,3-dien-4-yl)benzene

Base Information

Chemical Name:1-((Z)-deca-1,3-dien-4-yl)benzene
CAS No.:1316240-14-8
Molecular Formula:C₁₆H₂₂
Molecular Weight:214.351
Hs Code.:

Synonyms:1-((Z)-deca-1,3-dien-4-yl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((Z)-deca-1,3-dien-4-yl)benzene

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Technology Process of 1-((Z)-deca-1,3-dien-4-yl)benzene

There total 3 articles about 1-((Z)-deca-1,3-dien-4-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1316240-10-4
diphenyl (Z)-1-phenylbuta-1,3-dienyl phosphate

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 1316240-14-8
1-((Z)-deca-1,3-dien-4-yl)benzene

Guidance literature:: With palladium dichloride; In tetrahydrofuran; at 20 ℃; for 0.25h; stereoselective reaction;
DOI:10.1039/c1cc12052b

Reference yield:

: 932-88-7
1-iodo-2-phenylethyne

: 1316240-14-8
1-((Z)-deca-1,3-dien-4-yl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate / toluene / 4 h / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphate potassium salt / 1,4-dioxane

3: palladium dichloride / tetrahydrofuran / 0.25 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphate potassium salt; (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; palladium dichloride; In tetrahydrofuran; 1,4-dioxane; toluene; 3: Kumada-Corriu coupling reaction;
DOI:10.1039/c1cc12052b

Reference yield:

: 1316239-77-6
(Z)-2-iodo-1-phenylvinyl diphenyl phosphate

: 1316240-14-8
1-((Z)-deca-1,3-dien-4-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphate potassium salt / 1,4-dioxane

2: palladium dichloride / tetrahydrofuran / 0.25 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphate potassium salt; palladium dichloride; In tetrahydrofuran; 1,4-dioxane; 2: Kumada-Corriu coupling reaction;
DOI:10.1039/c1cc12052b