3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)thieno[2,3-b]pyridine-2-carboxamide

Base Information

Chemical Name:3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)thieno[2,3-b]pyridine-2-carboxamide
CAS No.:128991-36-6
Molecular Formula:C₁₃H₁₂N₄OS₂
Molecular Weight:304.396
Hs Code.:
Mol file:128991-36-6.mol

Synonyms:3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)-thieno[2,3-b]pyridine-2-carboxamide

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Chemical Property of 3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)thieno[2,3-b]pyridine-2-carboxamide

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Technology Process of 3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)thieno[2,3-b]pyridine-2-carboxamide

There total 5 articles about 3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)thieno[2,3-b]pyridine-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 7357-70-2
Cyanothioacetamide

: C₄H₃ClN₂OS

: 123-54-6,81235-32-7
acetylacetone

: 128991-36-6
3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)-thieno[2,3-b]pyridine-2-carboxamide

Guidance literature:: Cyanothioacetamide; acetylacetone; With sodium ethanolate; In N,N-dimethyl-formamide; at 20 - 50 ℃;

C₄H₃ClN₂OS; In N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1134/S1070428020060020

Reference yield: 80.0%

: 128991-34-4
2-(3-Cyano-4,6-dimethyl-pyridin-2-ylsulfanyl)-N-thiazol-2-yl-acetamide

: 128991-36-6
3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)-thieno[2,3-b]pyridine-2-carboxamide

Guidance literature:: With sodium ethanolate; In ethanol; for 0.25h; Heating;

Reference yield:

: 5448-49-7
2-chloro-N-(1,3-thiazol-2-yl)acetamide

: 128991-36-6
3-amino-4,6-dimethyl-N-(1,3-thiazol-2-yl)-thieno[2,3-b]pyridine-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / sodium acetate / ethanol / 0.5 h / Heating

2: 80 percent / NaOC₂H₅ / ethanol / 0.25 h / Heating

With sodium ethanolate; sodium acetate; In ethanol;