methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester

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Chemical Name:methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester
CAS No.:885328-58-5
Molecular Formula:C₃₄H₅₅N₃O₁₁S₂
Molecular Weight:745.956
Hs Code.:

Synonyms:methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester

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Chemical Property of methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester

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Technology Process of methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester

There total 3 articles about methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 885328-56-3
N,N'-dithiodi(4,1-phenylene)bis-(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanamide

: 20277-69-4
sodium methansulfinate

: 885328-58-5
methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester

Guidance literature:: With iodine; In dichloromethane; at 20 ℃;
DOI:10.1021/ol053049o

Reference yield:

: (S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propionic acid

: 885328-58-5
methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: HATU; DIPEA / dimethylsulfoxide; CH₂Cl₂ / 20 °C

1.2: 64 percent / dimethylsulfoxide; CH₂Cl₂

2.1: I₂ / CH₂Cl₂ / 20 °C

With iodine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ol053049o

Reference yield:

: 722-27-0
bis(4-aminophenyl)disulfide

: 885328-58-5
methanesulfonothioic acid S-[4-[(S)-2,3-bis[di(tert-butoxycarbonylmethyl)amino]propanylamino]phenyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: HATU; DIPEA / dimethylsulfoxide; CH₂Cl₂ / 20 °C

1.2: 64 percent / dimethylsulfoxide; CH₂Cl₂

2.1: I₂ / CH₂Cl₂ / 20 °C

With iodine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ol053049o