(S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide

Base Information

Chemical Name:(S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide
CAS No.:1007121-77-8
Molecular Formula:C₁₄H₁₉NO₅S
Molecular Weight:313.375
Hs Code.:

Synonyms:(S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide

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Chemical Property of (S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide

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Technology Process of (S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide

There total 1 articles about (S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 848777-16-2,186692-52-4
benzyl N-[(1S)-1-(hydroxymethyl)-2,2-dimethyl-propyl]carbamate

: 1007121-77-8
(S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide

Guidance literature:: ((S)-1-Hydroxymethyl-2,2-dimethyl-propyl)-carbamic acid benzyl ester; With thionyl chloride; In acetonitrile; at -40 ℃; for 0.0166667h;

With pyridine; In acetonitrile; at 20 ℃; for 1h;

With sodium periodate; water; ruthenium trichloride; In acetonitrile; Further stages.;
DOI:10.1021/ol702891p

Reference yield: 89.0%

: 1007121-77-8
(S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide

: 50487-71-3
4-methyl-N-(2-propenyl)benzenesulfonamide

: 1007121-83-6
benzyl (S)-1-(N-allyl-4-methylbenzenesulfonamido)-3,3-dimethylbutan-2-ylcarbamate

Guidance literature:: (S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide; 4-methyl-N-(2-propenyl)benzenesulfonamide; With potassium hydroxide; In acetonitrile;

With hydrogenchloride; In ethyl acetate; acetonitrile; Further stages.;
DOI:10.1021/ol702891p

Reference yield: 35.0%

: 1007121-77-8
(S)-3-(benzyloxycarbonyl)-4-tert-butyl-[1,2,3]oxathiazolidine 2,2-dioxide

: 73183-34-3
bis(pinacol)diborane

: (R)-benzyl (3,3-dimethyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-yl)carbamate

Guidance literature:: With copper(l) iodide; tetra-(n-butyl)ammonium iodide; triphenylphosphine; lithium tert-butoxide; In N,N-dimethyl-formamide; at 20 ℃; for 2h; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201501492