N-malonyl-2-amino-5-nitro-benzenesulfoximide

Base Information

Chemical Name:N-malonyl-2-amino-5-nitro-benzenesulfoximide
CAS No.:1086106-66-2
Molecular Formula:C₁₂H₁₅N₃O₆S
Molecular Weight:329.334
Hs Code.:

Synonyms:N-malonyl-2-amino-5-nitro-benzenesulfoximide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-malonyl-2-amino-5-nitro-benzenesulfoximide

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Technology Process of N-malonyl-2-amino-5-nitro-benzenesulfoximide

There total 6 articles about N-malonyl-2-amino-5-nitro-benzenesulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1086106-41-3
2-amino-5-nitrophenyl-S-methyl-sulfoximide

: 36239-09-5
ethyl chlorocarbonylacetate

: 1086106-66-2
N-malonyl-2-amino-5-nitro-benzenesulfoximide

Guidance literature:: In diethyl ether; N,N-dimethyl acetamide; at 20 ℃; for 16h;

Reference yield:

: 6310-41-4
N-(2-methylsulfanyl-phenyl)-acetamide

: 1086106-66-2
N-malonyl-2-amino-5-nitro-benzenesulfoximide

Guidance literature:: Multi-step reaction with 5 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.25 - 1.5 h / -30 °C / Cooling with acetonitrile/dry ice

2: sodium azide; sulfuric acid / chloroform / 20 - 40 °C

3: sodium nitrate; sulfuric acid / water

4: sodium hydroxide; water / 0.33 h / 100 °C

5: diethyl ether; N,N-dimethyl acetamide / 16 h / 20 °C

With sodium hydroxide; sodium nitrate; sodium azide; sulfuric acid; water; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; chloroform; N,N-dimethyl acetamide; water;

Reference yield:

: 501359-05-3
1,3-dimethyl-1λ⁴-benzo[e][1,2,4]thiadiazine 1-oxide

: 1086106-66-2
N-malonyl-2-amino-5-nitro-benzenesulfoximide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium nitrate; sulfuric acid / water

2: sodium hydroxide; water / 0.33 h / 100 °C

3: diethyl ether; N,N-dimethyl acetamide / 16 h / 20 °C

With sodium hydroxide; sodium nitrate; sulfuric acid; water; In diethyl ether; N,N-dimethyl acetamide; water;