tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>cyclohexylsilicate

Base Information

• Chemical Name: tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>cyclohexylsilicate
• CAS No.: 125764-09-2
• Molecular Formula: C₈H₂₀N*C₂₄H₁₉F₁₂O₂Si
• Molecular Weight: 725.733

Synonyms:tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>cyclohexylsilicate

Chemical Property of tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>cyclohexylsilicate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>cyclohexylsilicate

There total 1 articles about tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>cyclohexylsilicate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1-bromocyclohexane (108-85-0) + 3,3,3',3'-tetrakis(trifluoromethyl)-1,1'(3H,3'H)-spirobi<2,1-benzoxasilole> (70091-69-9) + tetraethylammonium bromide (71-91-0) → tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>cyclohexylsilicate (125764-09-2)

Guidance literature:

1-bromocyclohexane; With iodine; magnesium; In tetrahydrofuran; at 60 ℃; Inert atmosphere;

3,3,3',3'-tetrakis(trifluoromethyl)-1,1'(3H,3'H)-spirobi<2,1-benzoxasilole>; In tetrahydrofuran; Inert atmosphere; Reflux;

tetraethylammonium bromide; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1039/d0cc03286g

Reference yield: 98.0%

2-methylquinoline (91-63-4) + tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>cyclohexylsilicate (125764-09-2) → 4‐cyclohexyl‐2‐methylquinoline (37597-46-9)

Guidance literature:

With trifluoroacetic acid; 9-(2-mesityl)-10-methylacridinium perchlorate; In dichloromethane; at 23 ℃; for 24h; Schlenk technique; Inert atmosphere; Irradiation;

DOI:10.1039/d0cc03286g

Reference yield: 96.0%

ethyl coumarin-3-carboxylate (1846-76-0) + tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C2,O>cyclohexylsilicate (125764-09-2) → 4-cyclohexyl-3,4-dihydro-2-oxo-2H-1-benzopyran-3-carboxylic acid ethyl ester

Guidance literature:

With 3,6‐di‐tert‐butyl‐9‐mesityl‐10‐phenylacridin‐10‐ium tetrafluoroborate; In methanol; acetone; at 23 ℃; for 3h; Irradiation;

DOI:10.1002/chem.202005300

upstream raw materials:

1-bromocyclohexane

3,3,3',3'-tetrakis(trifluoromethyl)-1,1'(3H,3'H)-spirobi<2,1-benzoxasilole>

tetraethylammonium bromide

Downstream raw materials:

2-cyclohexyl-4-methylquinoline

4‐cyclohexyl‐2‐methylquinoline

2,4-dicyclohexylquinoline

methyl 1-cyclohexylisoquinoline-3-carboxylate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 125764-09-2 tetraethylammonium bis<α,α-bis(trifluoromethyl)benzenemethanolato(2-)-C²,O>cyclohexylsilicate

Send

Send

Metric Ton KG G Pound L ML

Send

Send