(E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester

Base Information

Chemical Name:(E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester
CAS No.:326496-55-3
Molecular Formula:C₁₅H₁₉BO₄
Molecular Weight:274.124
Hs Code.:

Synonyms:(E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester

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Chemical Property of (E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester

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Technology Process of (E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester

There total 5 articles about (E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 215876-82-7
2-(4-formylphenyl)-4,5-dimethyl-1,3,2-dioxaborolane

: 326496-55-3
(E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 20 ℃;
DOI:10.1002/1099-0690(200012)2000:23<3825::aid-ejoc3825>3.3.co;2-7

Reference yield:

: 34421-94-8
4-bromobenzaldehyde diethyl acetal

: 326496-55-3
(E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: nBuLi; B(O-iPr)3 / tetrahydrofuran; hexane / 20 °C

2: HCl; water / 7 h / 20 °C

3: 99 percent / MgSO₄ / ethyl acetate / 20 °C

4: LiCl; DBU / acetonitrile / 20 °C

With hydrogenchloride; n-butyllithium; Triisopropyl borate; water; magnesium sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In tetrahydrofuran; hexane; ethyl acetate; acetonitrile;
DOI:10.1002/1099-0690(200012)2000:23<3825::aid-ejoc3825>3.3.co;2-7

Reference yield:

: 87199-17-5
4-formylphenylboronic acid,

: 326496-55-3
(E)-3-[4-(4,5-Dimethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acrylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / MgSO₄ / ethyl acetate / 20 °C

2: LiCl; DBU / acetonitrile / 20 °C

With magnesium sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In ethyl acetate; acetonitrile;
DOI:10.1002/1099-0690(200012)2000:23<3825::aid-ejoc3825>3.3.co;2-7